反应条件
1: N-phenylmethylacetamide With pyridine; oxalyl dichloride; N, N-dibenzylacetamide in tetrahydrofuran
T=0°C; 1 h; Inert atmosphere;
2: With Propylene glycol in tetrahydrofuran
T=0 - 20°C; 2 h; Inert atmosphere;
3: benzyl chloroformate With potassium hydrogencarbonate in water; ethyl acetate
T=0°C; 16 h; Inert atmosphere;
参考文献
Koenig, Stefan G.; Vandenbossche, Charles P.; Zhao, Hang; Mousaw, Patrick; Singh, Surendra P.; Bakale, Roger P.
Organic Letters, 2009 , vol. 11, # 2 p. 433 - 436
