(2-溴-4-氟苯氧基)-乙酸合成路线 (共 5 条)
反应条件
hydrogenchloride in 1,4-dioxane
T=20°C; 12 h;
参考文献
Bolin, David Robert; Michoud, Christophe
Patent: US2006/178532 A1, 2006 ;
Location in patent: Page/Page column 13 ;
US 20060178532 A1
反应条件
1: carbon disulfide; bromine
2: aq. NaOH solution
View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,95, 97
反应条件
1: sulfuric acid; sodium nitrite; phosphoric acid / Erhitzen des Reaktionsgemisches mit Kupfer(II)-sulfat und wss. Schwefelsaeure auf 140grad
2: carbon disulfide; bromine
3: aq. NaOH solution
View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,95, 97
参考文献
Finger et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,95, 97
反应条件
tetrachloromethane; bromine; iodine
参考文献
Mel'nikow; Kukalenko
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 3708; engl. Ausg. S. 3664