全氟-2,2,3,3-四甲基丁烷合成路线 (共 6 条)
参考文献
Maraschin,N.J. et al.
Journal of the American Chemical Society, 1975 , vol. 97, p. 513 - 517
反应条件
moisture; Copper(I) trifluoromethanethiolate in acetonitrile
1.) -78 deg C, 2 h, 2.) from 55 deg C to 60 deg C, 4 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Munavalli, S.; Lewis, E. O.; Muller, A. J.; Rossman, D. I.; Rohrbaugh, D. K.; Ferguson, C. P.
Journal of Fluorine Chemistry, 1993 , vol. 63, # 3 p. 253 - 264
反应条件
moisture; Copper(I) trifluoromethanethiolate in acetonitrile
1.) -78 deg C, 2 h, 2.) from 55 deg C to 60 deg C, 4 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Munavalli, S.; Lewis, E. O.; Muller, A. J.; Rossman, D. I.; Rohrbaugh, D. K.; Ferguson, C. P.
Journal of Fluorine Chemistry, 1993 , vol. 63, # 3 p. 253 - 264
反应条件
in acetonitrile
1.) -78 deg C, 2 h, 2.) from 55 deg C to 60 deg C, 4 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Munavalli, S.; Lewis, E. O.; Muller, A. J.; Rossman, D. I.; Rohrbaugh, D. K.; Ferguson, C. P.
Journal of Fluorine Chemistry, 1993 , vol. 63, # 3 p. 253 - 264
反应条件
pyridine in various solvent(s)
recombination rate constant, various fluorine-containing radicals under different conditions; Rate constantMechanism;
参考文献
Tumanskii, B. L.; Bubnov, N. N.; Polishchuk, V. R.; Solodovnikov, S. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 10 p. 1821 - 1826
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 10 p. 2222 - 2227
反应条件
chlorine
T=201°C; 48 h;
参考文献
Tonelli, Claudio; Tortelli, Vito
Journal of Fluorine Chemistry, 1994 , vol. 67, # 2 p. 125 - 128