1-甲基-2-(苯氧基)苯合成路线 (共 45 条)
反应条件
caesium carbonate; copper(l) iodide in N,N-dimethyl-formamide
T=110°C; Ullmann condensation; 20 h;
参考文献
SALTIGO GMBH
Patent: US2009/143594 A1, 2009 ;
Location in patent: Page/Page column 4-5 ;
反应条件
aluminum oxide; potassium fluoride; copper(l) iodide; 1,10-phenanthroline
T=110°C; 14 h;
参考文献
Naidu, Ajay B.; Jaseer; Sekar, Govindasamy
Journal of Organic Chemistry, 2009 , vol. 74, # 10 p. 3675 - 3679
反应条件
1-methyl-pyrrolidin-2-one
T=120°C; Ullmann diaryl etherification; 5 h; Inert atmosphere;
参考文献
Mulla, Shafeek A.R.; Inamdar, Suleman M.; Pathan, Mohsinkhan Y.; Chavan, Santosh S.
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1826 - 1829
反应条件
caesium carbonate; copper(l) iodide in N,N-dimethyl-formamide
T=110°C; Ullmann condensation; 17 h;
参考文献
Rao, Honghua; Jin, Ying; Fu, Hua; Jiang, Yuyang; Zhao, Yufen
Chemistry - A European Journal, 2006 , vol. 12, # 13 p. 3636 - 3646
反应条件
[Ni0(1,5-cyclooctadiene)2]; caesium carbonate; dcype in anhydrous xylene
T=160°C; 72 h;
参考文献
Wang, Jiayi; Ferguson, Devin M.; Kalyani, Dipannita
Tetrahedron, 2013 , vol. 69, # 27-28 p. 5780 - 5790
反应条件
copper diacetate; triethylamine
T=20°C; 30 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Davan, Elham Etemadi; Rostami, Abed; Nematollahi, Arash
Journal of Organometallic Chemistry, 2013 , vol. 740, p. 123 - 130
反应条件
copper(I) oxide; caesium carbonate in tetrahydrofuran
T=150°C; Ullmann condensation; 3 h;
参考文献
Kim, Jee Young; Park, Ji Chan; Kim, Aram; Young Kim; Lee, Hyun Ju; Song, Hyunjoon; Park, Kang Hyun
European Journal of Inorganic Chemistry, 2009 , # 28 p. 4219 - 4223
反应条件
1: phenol With potassium tert-butylate in tetrahydrofuran
T=0°C; 0.25 h;
2: (o-Me-Ph)2IOTf in tetrahydrofuran
T=40°C; 0.5 h;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
Copper(I)chloride in chlorobenzene
参考文献
Rhone-Poulenc Industries
Patent: US4288386 A1, 1981 ;
反应条件
methyl pyridin-2-ylmethyl ketone; caesium carbonate; copper(I) bromide in dimethyl sulfoxide
T=150°C; 22 h; Inert atmosphere; chemoselective reaction;
参考文献
Zhang, Qi; Wang, Deping; Wang, Xianyang; Ding, Ke
Journal of Organic Chemistry, 2009 , vol. 74, # 18 p. 7187 - 7190