1-甲基-2-(苯氧基)苯合成路线 （共 45 条）
反应条件
dimethyl sulfoxide; potassium hydroxide
T=135°C; 48 h; Inert atmosphere;
参考文献
Yuan, Yu; Thome, Isabelle; Kim, Seok Hwan; Chen, Duanteng; Beyer, Astrid; Bonnamour, Julien; Zuidema, Erik; Chang, Sukbok; Bolm, Carsten
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 2892 - 2898
参考文献
Chan,K.C.; Huang,R.L.
Journal of the Chemical Society, 1965 , p. 2649 - 2651
反应条件
T=380 - 450°C; beim Leiten ueber ThO2;
参考文献
Sabatier; Mailhe
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1912 , vol. 155, p. 261
反应条件
1.) toluene, 20 deg C, 24 h, 2.) 220 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Sharutin; Sharutina; Osipov; Zhidkov; Muslin
Russian Journal of General Chemistry, 1997 , vol. 67, # 6 p. 973 - 974
反应条件
1.1: N,N,N',N,-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 - 20 °C / |Inert atmosphere
1.2: 12 h / 20 °C / |Inert atmosphere
2.1: ammonium chloride / water
3.1: palladium diacetate; potassium carbonate; iodine / acetonitrile / 12 h / 20 - 80 °C / |Schlenk technique; |Inert atmosphere; |Sealed tube
View Scheme
参考文献
Niu, Liting; Yang, Haijun; Jiang, Yuyang; Fu, Hua
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3625 - 3632
