4-(4-吗啉基)苯乙酮合成路线 （共 16 条）
反应条件
potassium tert-butylate in ethylene glycol dimethyl ether T=50°C; Hartwig-Buchwald amination; 20 h; Inert atmosphere;
参考文献
Mennecke, Klaas; Kirschning, Andreas
Synthesis, 2008 , # 20 p. 3267 - 3272
反应条件
lithium hexamethyldisilazane; Verkade nonionic superbase; palladium diacetate in tetrahydrofuran; toluene T=80°C; 30 h;
参考文献
Urgaonkar, Sameer; Verkade, John G.
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 6 p. 611 - 616
参考文献
Tian, Wei
Patent: US2003/171581 A1, 2003 ;
反应条件
2-(dicyclohexylphosphino)-4'-(N,N-dimethylamino)-1,1'-biphenyl T=100°C;
参考文献
Pratap, Ramendra; Parrish, Damon; Gunda, Padmaja; Venkataraman; Lakshman, Mahesh K.
Journal of the American Chemical Society, 2009 , vol. 131, # 34 p. 12240 - 12249
反应条件
potassium hydroxide; Pd[P(t-Bu3)]2; N-hexadecyl-N,N,N-trimethylammonium bromide in water; toluene T=90°C; 6 h;
参考文献
Kuwano, Ryoichi; Utsunomiya, Masaru; Hartwig, John F.
Journal of Organic Chemistry, 2002 , vol. 67, # 18 p. 6479 - 6486
反应条件
palladium 10 on activated carbon; sodium t-butanolate; 2-dicyclohexylphosphino-1,1'-biphenyl in tert-butyl alcohol T=80°C; Buchwald-Hartwig amination; Inert atmosphere;
参考文献
Komaromi, Anna; Novak, Zoltan
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 9 p. 1523 - 1532
反应条件
potassium carbonate in water T=100°C; 1 h; Microwave irradiationGreen chemistry;
参考文献
Li, Hong Bo; Liang, Wu; Ma, Chang Peng; Kai, Yong Mao; Li, Lei; Zhang, Yong Gang
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 4 p. 995 - 998
反应条件
ruthenium(II)-carbonyl-tris(triphenylphosphine) dihydride; oct-1-ene; dcype in dimethyl sulfoxide T=115°C; 24 h; Inert atmosphere; Reagent/catalyst;
参考文献
Watson, Andrew J. A.; Atkinson, Benjamin N.; Maxwell, Aoife C.; Williams, Jonathan M. J.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 734 - 740
反应条件
sulfur T=100°C; 1 h; Irradiationneat (no solvent);
参考文献
Valdez-Rojas, Jose Ernesto; Rios-Guerra, Hulme; Ramirez-Sanchez, Alma Leticia; Garcia-Gonzalez, Guadalupe; Alvarez-Toledano, Cecilio; Lopez-Cortes, Jose Guadalupe; Toscano, Ruben A.; Penieres-Carrillo, Jose Guillermo
Canadian Journal of Chemistry, 2012 , vol. 90, # 7 p. 567 - 573
参考文献
Terpugova,M.P. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1976 , vol. 25, p. 650 - 651
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1976 , vol. 25, p. 665 - 666
