lithium aluminium tetrahydride in diethyl ether
a.) reflux while adding reagent b.) room temperature overnight c.) 30 min reflux;
参考文献
Vig, O. P.; Sharma, M. L.; Taneja, K. C.; Malik, Neera
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 10 p. 863 - 865
1: 90 percent / LiAlH4 / diethyl ether / a.) reflux while adding reagent b.) room temperature overnight c.) 30 min reflux
2: 70 percent / pyridinium chlorochromate, NaOAc / CH2Cl2 / 3 h
View Scheme
参考文献
Vig, O. P.; Sharma, M. L.; Taneja, K. C.; Malik, Neera
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 10 p. 863 - 865
