hydrogenchloride; 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane Multistep reaction;

triethylamine in dichloromethane T=0 - 30°C; 2 h;

acetic anhydride in pyridine; water; ethyl acetate

triethylamine in dichloromethane T=20°C; 16 h;

暂无反应条件数据

1: di-tert-butyl dicarbonate; 3-bromobenzylamine hydrochloride With sodium hydrogencarbonate in 1,4-dioxane; water T=20°C; 24 h; 2: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 3: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - -15°C; 1.5 h;