in water-d2 byproducts: ND3; heating educts in closed pyrex glass tube at 180°C, 3h;; separation of ND3; evapn. at 110°C; dissoln. in H2O; treating with active coal;;
Bartholomew, Richard J.; Stevenson, Wendy J.; Irish, Donald E.
Spectrochimica Acta - Part A Molecular Spectroscopy, 1996 , vol. 52, # 13 p. 1695 - 1701
in neat (no solvent) distillation of DCOONa with an excess of D3PO4;;
参考文献
Ropp, G. A.; Melton, C. E.
Journal of the American Chemical Society, 1958 , vol. 80, p. 3509 - 3512
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Gmelin Handbook: C: MVol.C4, 5.1.4, page 50 - 51
