2-(3-甲基苯基)硫基乙酸合成路线 （共 13 条）
反应条件
1: Br2 / acetic acid 2: aq. H2O2, aq. H2SO4 View Scheme
参考文献
Walker,D.; Leib,J.
Journal of Organic Chemistry, 1962 , vol. 27, p. 4455 - 4461
反应条件
tris(2,2'-bipyridine)chromium(III) in acetonitrile T=24.9°C; Irradiationother reag.; Rate constant;
参考文献
Gnanaraj; Rajagopal; Srinivasan
Tetrahedron, 1994 , vol. 50, # 31 p. 9447 - 9456
反应条件
1: aq. H2O2 / acetic acid 2: aq. H2O2 / acetic acid View Scheme
参考文献
Kenney,W. et al.
Journal of the American Chemical Society, 1961 , vol. 83, p. 4019 - 4022
反应条件
perchloric acid; NaBO3; acetic acid T=24.9°C; var. temp., ΔH(excit.), ΔS(excit.); Rate constantThermodynamic dataMechanism;
参考文献
Kabilan, S.; Pandiarajan, K.; Krishnasamy, K.; Sankar, P.
International Journal of Chemical Kinetics, 1995 , vol. 27, # 5 p. 443 - 452
反应条件
perchloric acid; pyridinium chlorochromate in water; acetic acid T=24.85 - 44.85°C; Oxidation; Kinetics;
参考文献
Kabilan; Girija; Rajagopal
International Journal of Chemical Kinetics, 1999 , vol. 31, # 10 p. 683 - 688
反应条件
perchloric acid; NaBO3; acetic acid T=24.9°C; var. temp., ΔH(excit.), ΔS(excit.); Rate constantThermodynamic dataMechanism;
参考文献
Kabilan, S.; Pandiarajan, K.; Krishnasamy, K.; Sankar, P.
International Journal of Chemical Kinetics, 1995 , vol. 27, # 5 p. 443 - 452
反应条件
carbon disulfide; hydrogen fluoride Erhitzen des Reaktionsprodukts in Essigsaeure mit Zink und wss. Salzsaeure;
参考文献
Tarbell; Fukushima
Journal of the American Chemical Society, 1946 , vol. 68, p. 1456,1458
Organic Syntheses, 1955 , vol. Coll. Vol. III, p. 809
参考文献
Behaghel
Journal fuer Praktische Chemie (Leipzig), 1926 , vol. <2> 114, p. 298
反应条件
1: 3-methylbenzenethiol With sodium hydroxide in water
2: sodium salt of the chloroacetic acid in water
T=20°C; 4 h; Reflux;
3: With hydrogenchloride in water
T=20°C; pH=2;
参考文献
Okaecwe, Thokozile; Swanepoel, Abraham J.; Petzer, Anel; Bergh, Jacobus J.; Petzer, Jacobus P.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 14 p. 4336 - 4347
反应条件
n-butyllithium
Yield given. Multistep reaction;
参考文献
Cabiddu, Salvatore; Fattuoni, Claudia; Floris, Costantino; Gelli, Gioanna; Melis, Stefana; Sotgiu, Francesca
Tetrahedron, 1990 , vol. 46, # 3 p. 861 - 884
