2-(3-甲基苯基)硫基乙酸合成路线 (共 13 条)
反应条件
1.1: n-butyllithium / hexane; diethyl ether / 2 h / 0 °C
1.2: 77 percent / diethyl ether; hexane / 0 - 20 °C
2.1: 0.59 g / n-butyllithium / hexane; diethyl ether / 0 - 20 °C
View Scheme
参考文献
Cabiddu, Maria G.; Cabiddu, Salvatore; Cadoni, Enzo; De Montis, Stefania; Fattuoni, Claudia; Melis, Stefana
Tetrahedron, 2004 , vol. 60, # 17 p. 3915 - 3920
反应条件
ammonium cerium(IV) nitrate in water; acetic acid
T=25 - 45°C; ΔH(excit.), ΔS(excit.); KineticsThermodynamic data;
参考文献
Gurumurthy, Rajagopala; Gopalakhrishnan, Mannathusamy; Sathiyanarayanan, Kulathu Iyer
Tetrahedron, 1994 , vol. 50, # 48 p. 13731 - 13738
反应条件
1: dihydrogen peroxide
2: chromic acid / acetonitrile; water / 10 - 30 °C
View Scheme
参考文献
Subramaniam, Perumal; Selvi, Natesan Thamil; Devi, Soundarapandian Sugirtha
Journal of the Korean Chemical Society, 2014 , vol. 58, # 1 p. 17 - 24