1-戊基-4-[2-(4-甲氧苯基)乙炔基]苯合成路线 (共 2 条)
反应条件
1: methoxybenzene With air; Bi(NO3)3·5H2O; iodine; bismuth(III) chloride in acetonitrile T=20°C; 6 h; 2: 4-n-pentyl-phenylacetylene With piperidine; bis-triphenylphosphine-palladium(II) chloride in acetonitrile T=70°C; 3 h;
参考文献
Wan, Shun; Wang, Sunewang R.; Lu, Wenjun
Journal of Organic Chemistry, 2006 , vol. 71, # 11 p. 4349 - 4352
反应条件
tetrabutylammomium bromide; potassium acetate; cyclopalladated ferrocenylimine in N,N-dimethyl acetamide T=80°C; Sonogashira coupling; 24 h;
参考文献
Yang, Fan; Cui, Xiuling; Li, Ya-nan; Zhang, Jinli; Ren, Ge-rui; Wu, Yangjie
Tetrahedron, 2007 , vol. 63, # 9 p. 1963 - 1969