5-乙酰基-2-甲氧基苯甲酸甲酯合成路线 (共 7 条)
反应条件
sodium carbonate in N,N-dimethyl-formamide
参考文献
Institute of Medicinal Molecular Design, Inc.
Patent: EP1510207 A1, 2005 ;
Location in patent: Page/Page column 131 ;
EP 1510207 A1
Title/Abstract Full Text Show Details
Institute of Medicinal Molecular Design, Inc.
Patent: EP1510210 A1, 2005 ;
Location in patent: Page/Page column 131 ;
反应条件
caesium carbonate; methyl iodide in N,N-dimethyl-formamide
参考文献
Sharma, Shalini; von Borstel, Reid W.
Patent: US2003/149107 A1, 2003 ;
反应条件
hydrogenchloride; potassium carbonate in N,N-dimethyl-formamide
参考文献
The Upjohn Company
Patent: US5502187 A1, 1996 ;
反应条件
1: NaOH-solution
2: diethyl ether
View Scheme
参考文献
v. Krannichfeldt
Chemische Berichte, 1914 , vol. 47, p. 157
参考文献
v. Krannichfeldt
Chemische Berichte, 1914 , vol. 47, p. 157
反应条件
iron(III) chloride
1) THF, -78 deg C, 3 h, 2) r.t., 20 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kauffmann, Thomas; Voss, Karl-Uwe; Neiteler, Gabriele
Chemische Berichte, 1993 , vol. 126, # 6 p. 1453 - 1460
参考文献
Singh, Rajendra; Zhou, Haihong
Patent: US2002/164649 A1, 2002 ;