2-乙酰-7-羟基苯并呋喃合成路线 （共 17 条）
反应条件
potassium carbonate in acetone
T=54°C; 2 h;
参考文献
Ando, Kumiko; Tsuji, Eriko; Ando, Yuko; Kunitomo, Jun-Ichi; Kobayashi, Reina; Yokomizo, Takehiko; Shimizu, Takao; Yamashita, Masayuki; Ohta, Shunsaku; Nabe, Takeshi; Kohno, Shigekatsu; Ohishi, Yoshitaka
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 11 p. 2129 - 2139
反应条件
1: 93.3 percent / AlCl3; Br2 / CH2Cl2 / 3 h / 26 °C
2: 78.9 percent / K2CO3 / acetone / 2 h / 54 °C
View Scheme
参考文献
Ando, Kumiko; Tsuji, Eriko; Ando, Yuko; Kunitomo, Jun-Ichi; Yamashita, Masayuki; Ohta, Shunsaku; Nabe, Takeshi; Kohno, Shigekatsu; Yokomizo, Takehiko; Shimizu, Takao; Ohishi, Yoshitaka
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3427 - 3431
反应条件
1: 93.3 percent / AlCl3; Br2 / CH2Cl2 / 3 h / 26 °C
2: 67.8 percent / K2CO3 / acetone / 2 h / 54 °C
View Scheme
参考文献
Ando, Kumiko; Tsuji, Eriko; Ando, Yuko; Kunitomo, Jun-Ichi; Yamashita, Masayuki; Ohta, Shunsaku; Nabe, Takeshi; Kohno, Shigekatsu; Yokomizo, Takehiko; Shimizu, Takao; Ohishi, Yoshitaka
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3427 - 3431
反应条件
1: 61.4 percent / K2CO3 / acetone / 2 h / 54 °C
2: 77.9 percent / HNO3 / acetic anhydride / 1 h / 26 °C
View Scheme
参考文献
Ando, Kumiko; Tsuji, Eriko; Ando, Yuko; Kuwata, Noriko; Kunitomo, Jun-Ichi; Yamashita, Masayuki; Ohta, Shunsaku; Kohno, Shigekatsu; Ohishi, Yoshitaka
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 4 p. 625 - 635
参考文献
Kaken Pharmaceutical Co., Ltd.
Patent: US4666931 A1, 1987 ;
参考文献
Ohishi; Mukai; Nagahara; Yajima; Kajikawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 9 p. 2398 - 2405
反应条件
sodium hydroxide in ethanol; cyclohexane; ethyl acetate; Petroleum ether
参考文献
Kakenyaku Kako Co., Ltd.
Patent: US4056626 A1, 1977 ;
US 4056626 A
