1,4-二氢-4-氧代-7-(4-吡啶基)喹啉-3-羧酸乙酯合成路线 (共 5 条)
反应条件
in various solvent(s)
0.2 h; Heatingheating in Dowtherm;
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
1: 91 percent / 0.13 h / 130 °C
2: 75 percent / various solvent(s) / 0.2 h / Heating; heating in Dowtherm
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
1: 91 percent / 0.13 h / 130 °C
2: 75 percent / various solvent(s) / 0.2 h / Heating; heating in Dowtherm
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
potassium carbonate in N,N-dimethyl-formamide
1) 60 deg C, 15 min; 2) stirring 1 h;;
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
1: 45 percent / 1) potassium carbonate / dimethylformamide / 1) 60 deg C, 15 min; 2) stirring 1 h;
2: 89 percent / aq. 10percent KOH / 1 h / Heating
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863