7-(2,6-二甲基-4-吡啶基)-1,4-二氢-4-氧代喹啉-3-羧酸乙酯合成路线 （共 5 条）
反应条件
in various solvent(s)
0.2 h; Heatingheating in Dowtherm;
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
1: 78 percent / 0.13 h / 130 °C
2: 85 percent / various solvent(s) / 0.2 h / Heating; heating in Dowtherm
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
1: 78 percent / 0.13 h / 130 °C
2: 85 percent / various solvent(s) / 0.2 h / Heating; heating in Dowtherm
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
potassium carbonate in N,N-dimethyl-formamide
1) 60 deg C, 15 min; 2) stirring 1 h;;
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
1: 65 percent / 1) potassium carbonate / dimethylformamide / 1) 60 deg C, 15 min; 2) stirring 1 h;
2: 24 percent / aq. 10percent KOH / 1 h / Heating
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
