反应条件
1: 9-bromo-10-(9,9-dimethyl-9H-fluoren-2-yl)anthracene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; Inert atmosphere;
2: boric acid trimethyl ester in tetrahydrofuran; hexane
T=20°C;
3: With hydrogenchloride; water in tetrahydrofuran; hexane
参考文献
Shin, Hyo Nim; Kim, Chi Sik; Kwon, Hyuck Joo; Cho, Young Jung; Kim, Bong Ok; Kim, Sung Min; Yoon, Seung Soo
Patent: US2011/152587 A1, 2011 ;
Location in patent: Page/Page column 31 ;