N-(4-氯苄基)异丙基胺合成路线 (共 6 条)
反应条件
[(C5Me5)IrI2]2 in anhydrous xylene
T=155°C; 10 h; Inert atmosphere;
参考文献
Saidi, Ourida; Williams, Jonathan M. J.; Blacker, A. John; Farah, Mohamed M.; Marsden, Stephen P.
Angewandte Chemie, International Edition, 2009 , vol. 48, # 40 p. 7375 - 7378
Angewandte Chemie, 2009 , vol. 121, # 40 p. 7511 - 7514
反应条件
lithium aluminium tetrahydride in diethyl ether
Reflux;
参考文献
Stankovic, Sonja; D'Hooghe, Matthias; De Kimpe, Norbert
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 19 p. 4266 - 4273
反应条件
sodium hydrogencarbonate in glycerol
5 h; Heating;
参考文献
Galin, F. Z.; Ignatyuk, V. K.; Rakhimov, R. G.; Amirkhanov, D. V.; Poskryakov, A. V.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 7.2 p. 1555 - 1557
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , vol. 38, # 7 p. 1694 - 1696
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=160°C; Microwave irradiation; regioselective reaction;
参考文献
Stankovic, Sonja; D'Hooghe, Matthias; De Kimpe, Norbert
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 19 p. 4266 - 4273
参考文献
Hao, Wei; Fujii, Takayoshi; Dong, Tiaoling; Wakai, Youko; Yoshimura, Toshiaki
Heteroatom Chemistry, 2004 , vol. 15, # 3 p. 193 - 198
反应条件
1: 45 percent / Et3N / 2-ethoxy-ethanol / 1 h / Heating
2: 97 percent / Fe, conc. aq. HCl / 1 h / Heating
3: 10 percent / bis-(2-methoxy-ethyl) ether / 0.75 h / 145 °C
View Scheme
参考文献
Colbry, Norman L.; Elslager, Edward F.; Werbel, Leslie M.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 2 p. 248 - 252