4-氨基联苯-3-羧酸甲酯合成路线 （共 4 条）
反应条件
hydrogen; palladium 10 on activated carbon in ethyl acetate P=1551.49 Torr; 4 h;
参考文献
WO2005/85177 A2, ;
Page/Page column 48-49 ;
反应条件
1: thionyl chloride / 70 °C 2: palladium 10 on activated carbon; hydrogen / methanol / 15 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 4 p. 1557 - 1568
反应条件
1.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 48 h / Inert atmosphere; Reflux 1.2: pH 3 2.1: thionyl chloride / 70 °C 3.1: palladium 10 on activated carbon; hydrogen / methanol / 15 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 4 p. 1557 - 1568
反应条件
1.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 48 h / Inert atmosphere; Reflux 1.2: pH 3 2.1: thionyl chloride / 70 °C 3.1: palladium 10 on activated carbon; hydrogen / methanol / 15 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 4 p. 1557 - 1568
