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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
间溴三氟甲苯
合成路线
（共 228 条）
401-78-5
间溴三氟甲苯
+
106-38-7
对溴甲苯
→
反应条件
613-33-2
4,4'-二甲基联苯
+
97067-19-1
反应条件
1: para-bromotoluene With magnesium in diethyl ether 2: 1-bromo-3-trifluoromethyl-benzene in diethyl ether Kumada coupling reaction; 3 h; Reflux;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 2 p. 331 - 335
401-78-5
间溴三氟甲苯
→
反应条件
365426-92-2
反应条件
1: 93 percent / aq. Na2CO3; Pd(PPh3)4 / ethanol; toluene / 3 h / Heating 2: 82 percent / aq. HI / 7.5 h / Heating View Scheme
参考文献
Mor, Marco; Rivara, Silvia; Lodola, Alessio; Plazzi, Pier Vincenzo; Tarzia, Giorgio; Duranti, Andrea; Tontini, Andrea; Piersanti, Giovanni; Kathuria, Satish; Piomelli, Daniele
Journal of Medicinal Chemistry, 2004 , vol. 47, # 21 p. 4998 - 5008
106-39-8
4-溴氯苯
+
401-78-5
间溴三氟甲苯
→
反应条件
19482-11-2
+
97067-19-1
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; Negishi cross-coupling; 6 h; Inert atmosphere;
参考文献
Dong, Zhi-Bing; Manolikakes, Georg; Shi, Lei; Knochel, Paul; Mayr, Herbert
Chemistry - A European Journal, 2010 , vol. 16, # 1 p. 248 - 253
401-78-5
间溴三氟甲苯
+
2786-01-8
→
反应条件
402-43-7
对溴三氟甲苯
+
368-49-0
反应条件
in tetrahydrofuran; biphenyl; pentane T=-75.16°C; Inert atmosphere; Equilibrium constant;
参考文献
Gorecka-Kobylinska, Joanna; Schlosser, Manfred
Journal of Organic Chemistry, 2009 , vol. 74, # 1 p. 222 - 229
401-78-5
间溴三氟甲苯
+
100-01-6
对硝基苯胺
→
反应条件
369-90-4
反应条件
tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in toluene T=100°C; 9 h; Inert atmosphere;
参考文献
Takeuchi, Tomoki; Oishi, Shinya; Kaneda, Masato; Misu, Ryosuke; Ohno, Hiroaki; Sawada, Jun-Ichi; Asai, Akira; Nakamura, Shinya; Nakanishi, Isao; Fujii, Nobutaka
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 12 p. 3171 - 3179
401-78-5
间溴三氟甲苯
+
98-80-6
苯硼酸
→
反应条件
366-04-1
3-(三氟甲基)联苯
反应条件
potassium phosphate in water; N,N-dimethyl-formamide T=100°C; Suzuki-Miyaura reaction; 0.5 h;
参考文献
Wu, Qinxu; Wu, Leilei; Zhang, Lei; Fu, Haiyan; Zheng, Xueli; Chen, Hua; Li, Ruixiang
Tetrahedron, 2014 , vol. 70, # 21 p. 3471 - 3477
401-78-5
间溴三氟甲苯
+
2633-57-0
(三-2-丙烯-1-基硅烷基)-苯
→
反应条件
366-04-1
3-(三氟甲基)联苯
反应条件
tetrabutyl ammonium fluoride; palladium dichloride; tri-cyclo-hexyl-phosphine in water; dimethyl sulfoxide T=80°C; 2 h;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
401-78-5
间溴三氟甲苯
+
129393-76-6
→
反应条件
366-04-1
3-(三氟甲基)联苯
反应条件
trifuran-2-yl-phosphane; tetrabutyl ammonium fluoride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in 1-methyl-pyrrolidin-2-one T=100°C; 9 h;
参考文献
Nakamura, Tomoaki; Kinoshita, Hidenori; Shinokubo, Hiroshi; Oshima, Koichiro
Organic Letters, 2002 , vol. 4, # 18 p. 3165 - 3167
401-78-5
间溴三氟甲苯
+
780-69-8
→
反应条件
366-04-1
3-(三氟甲基)联苯
反应条件
N,N-bis(indolin-1-yl)ethane-1,2-diimine; tetrabutyl ammonium fluoride; palladium dichloride in tetrahydrofuran; toluene T=80°C; Hiyama cross-coupling; 3 h;
参考文献
Mino, Takashi; Shirae, Yoshiaki; Saito, Takeshi; Sakamoto, Masami; Fujita, Tsutomu
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9499 - 9502
401-78-5
间溴三氟甲苯
+
143-66-8
→
反应条件
366-04-1
3-(三氟甲基)联苯
反应条件
MCM-41-supported thioether palladium(0) in N,N-dimethyl-formamide T=120°C; Suzuki coupling; 10 h;
参考文献
Li, Jianying; Huang, Yixiang; Cai, Mingzhong
Journal of Chemical Research, 2006 , # 10 p. 658 - 660
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