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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4,7-喹啉二胺
合成路线
（共 9 条）
40107-14-0
→
反应条件
40107-15-1
4,7-喹啉二胺
反应条件
hydrogenchloride; tin(ll) chloride in water; acetic acid T=60°C; 2 h;
参考文献
Nsumiwa, Samkele; Kuter, David; Wittlin, Sergio; Chibale, Kelly; Egan, Timothy J.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 13 p. 3738 - 3748
99-09-2
间硝基苯胺
→
反应条件
40107-15-1
4,7-喹啉二胺
反应条件
1: ethanol / 2 h / 90 °C 2: diphenylether / |Reflux 3: trichlorophosphate / 0.5 h / 140 °C 4: ammonium hydroxide; zinc(II) chloride / 70 °C 5: tin(ll) chloride; hydrogenchloride / water; acetic acid / 2 h / 60 °C View Scheme
参考文献
Nsumiwa, Samkele; Kuter, David; Wittlin, Sergio; Chibale, Kelly; Egan, Timothy J.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 13 p. 3738 - 3748
40107-10-6
二乙基(3-硝基苯胺亚甲基)丙二酸
→
反应条件
40107-15-1
4,7-喹啉二胺
反应条件
1: diphenylether / 1 h / |Reflux 2: sodium hydroxide / water / 0.75 h / |Reflux 3: ammonium hydroxide / water / 16 h / 100 °C 4: diphenylether / 0.75 h / |Reflux 5: trichlorophosphate / 0.5 h / 140 °C 6: ammonium hydroxide; zinc(II) chloride / 70 °C 7: tin(ll) chloride; hydrogenchloride / water; acetic acid / 2 h / 60 °C View Scheme
参考文献
Nsumiwa, Samkele; Kuter, David; Wittlin, Sergio; Chibale, Kelly; Egan, Timothy J.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 13 p. 3738 - 3748
7248-88-6
4-羟基-7-硝基喹啉-3-羧酸乙酯
→
反应条件
40107-15-1
4,7-喹啉二胺
反应条件
1: sodium hydroxide / water / 0.75 h / |Reflux 2: ammonium hydroxide / water / 16 h / 100 °C 3: diphenylether / 0.75 h / |Reflux 4: trichlorophosphate / 0.5 h / 140 °C 5: ammonium hydroxide; zinc(II) chloride / 70 °C 6: tin(ll) chloride; hydrogenchloride / water; acetic acid / 2 h / 60 °C View Scheme
参考文献
Nsumiwa, Samkele; Kuter, David; Wittlin, Sergio; Chibale, Kelly; Egan, Timothy J.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 13 p. 3738 - 3748
40107-11-7
→
反应条件
40107-15-1
4,7-喹啉二胺
反应条件
1: ammonium hydroxide / water / 16 h / 100 °C 2: diphenylether / 0.75 h / |Reflux 3: trichlorophosphate / 0.5 h / 140 °C 4: ammonium hydroxide; zinc(II) chloride / 70 °C 5: tin(ll) chloride; hydrogenchloride / water; acetic acid / 2 h / 60 °C View Scheme
参考文献
Nsumiwa, Samkele; Kuter, David; Wittlin, Sergio; Chibale, Kelly; Egan, Timothy J.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 13 p. 3738 - 3748
6270-14-0
4-羟基-7-硝基喹啉
→
反应条件
40107-15-1
4,7-喹啉二胺
反应条件
1: trichlorophosphate / 0.5 h / 140 °C 2: ammonium hydroxide; zinc(II) chloride / 70 °C 3: tin(ll) chloride; hydrogenchloride / water; acetic acid / 2 h / 60 °C View Scheme
参考文献
Nsumiwa, Samkele; Kuter, David; Wittlin, Sergio; Chibale, Kelly; Egan, Timothy J.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 13 p. 3738 - 3748
18436-76-5
4-氯-7-硝基喹啉
→
反应条件
40107-15-1
4,7-喹啉二胺
反应条件
1: ammonium hydroxide; zinc(II) chloride / 70 °C 2: tin(ll) chloride; hydrogenchloride / water; acetic acid / 2 h / 60 °C View Scheme
参考文献
Nsumiwa, Samkele; Kuter, David; Wittlin, Sergio; Chibale, Kelly; Egan, Timothy J.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 13 p. 3738 - 3748
40107-12-8
→
反应条件
40107-15-1
4,7-喹啉二胺
反应条件
1: diphenylether / 0.75 h / |Reflux 2: trichlorophosphate / 0.5 h / 140 °C 3: ammonium hydroxide; zinc(II) chloride / 70 °C 4: tin(ll) chloride; hydrogenchloride / water; acetic acid / 2 h / 60 °C View Scheme
参考文献
Nsumiwa, Samkele; Kuter, David; Wittlin, Sergio; Chibale, Kelly; Egan, Timothy J.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 13 p. 3738 - 3748
25063-48-3
→
反应条件
40107-15-1
4,7-喹啉二胺
反应条件
1: diphenylether / |Reflux 2: trichlorophosphate / 0.5 h / 140 °C 3: ammonium hydroxide; zinc(II) chloride / 70 °C 4: tin(ll) chloride; hydrogenchloride / water; acetic acid / 2 h / 60 °C View Scheme
参考文献
Nsumiwa, Samkele; Kuter, David; Wittlin, Sergio; Chibale, Kelly; Egan, Timothy J.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 13 p. 3738 - 3748
