N,N’-二异丙基乙二胺合成路线 （共 14 条）
反应条件
in Petroleum ether stoich. amt., room temp. under nitrogene; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
1: With hydrogenchloride in 1,4-dioxane
T=0 - 20°C; 2 h;
2: With formic acid in 1,4-dioxane
T=100°C; 16 h; Product distribution / selectivity;
参考文献
GREENCENTRE CANADA; BARRY, Sean; COYLE, Jason; CLARK, Timothy James; HASTIE, Jeffrey J.M.
Patent: WO2012/155264 A1, 2012 ;
Location in patent: Page/Page column 51 ;
参考文献
Shepherd,R.G.; Wilkinson,R.G.
Journal of Medicinal and Pharmaceutical Chemistry, 1962 , vol. 5, p. 823 - 835
反应条件
formic acid in water
Eschweiler-Clarke reaction; 16 h; Heating;
参考文献
Bilke, Julia L.; O'Brien, Peter
Journal of Organic Chemistry, 2008 , vol. 73, # 16 p. 6452 - 6454
