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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-(4-氯苯基)噻吩
合成路线
（共 24 条）
106-39-8
4-溴氯苯
+
5713-61-1
苯硫基溴化镁
→
反应条件
492-97-7
2,2'-联二噻吩
+
40133-23-1
2-(4-氯苯基)噻吩
反应条件
triphenylphosphine; Pd bipyridyl anchored nanosized mesoporous silica MCM-41 in tetrahydrofuran Kumada-Corriu reaction; 36 h; Heating;
参考文献
Tsai, Fu-Yu; Lin, Bo-Nan; Chen, Ming-Jie; Mou, Chung-Yuan; Liu, Shiuh-Tzung
Tetrahedron, 2007 , vol. 63, # 20 p. 4304 - 4309
3437-95-4
2-碘噻吩
+
195062-61-4
4-氯苯硼酸频哪醇酯
→
反应条件
40133-23-1
2-(4-氯苯基)噻吩
反应条件
potassium carbonate in methanol T=60°C; Suzuki-Miyaura Coupling; 1 h;
参考文献
Pandarus, Valerica; Desplantier-Giscard, Delphine; Gingras, Genevieve; Ciriminna, Rosaria; Demma Cara, Piera; Beland, Francois; Pagliaro, Mario
Tetrahedron Letters, 2013 , vol. 54, # 35 p. 4712 - 4716
6165-68-0
2-噻吩硼酸
→
反应条件
40133-23-1
2-(4-氯苯基)噻吩
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in water T=85°C; Suzuki Coupling; 3 h; Inert atmosphere;
参考文献
Reddy, Vutukuri Prakash; Qiu, Renhua; Iwasaki, Takanori; Kambe, Nobuaki
Organic Letters, 2013 , vol. 15, # 6 p. 1290 - 1293
188290-36-0
+
673-41-6
→
反应条件
40133-23-1
2-(4-氯苯基)噻吩
反应条件
potassium acetate; 18-crown-6 ether 1.5 h; Ambient temperature;
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
1003-09-4
2-溴噻吩
+
873-77-8
4-氯苯基溴化镁
→
反应条件
2050-68-2
4,4'-二氯联苯
+
492-97-7
2,2'-联二噻吩
+
40133-23-1
2-(4-氯苯基)噻吩
反应条件
1: 4-chlorophenyl-magnesium bromide With bismuth(III) chloride 2: thien-2-yl bromide With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
91193-23-6
→
反应条件
40133-23-1
2-(4-氯苯基)噻吩
反应条件
1: didodecanoyl peroxide / ethyl acetate / |Inert atmosphere; |Reflux 2: titanium tetrachloride / dichloromethane / 0 - 20 °C / |Inert atmosphere 3: silica gel / neat (no solvent) / 215 °C / |Inert atmosphere View Scheme
参考文献
Jullien, Helene; Quiclet-Sire, Beatrice; Tetart, Thomas; Zard, Samir Z.
Organic Letters, 2014 , vol. 16, # 1 p. 302 - 305
188290-36-0
→
反应条件
40133-23-1
2-(4-氯苯基)噻吩
反应条件
sodium hydroxide
参考文献
Gomberg; Bachmann
Journal of the American Chemical Society, 1924 , vol. 46, p. 2343
Journal of the American Chemical Society, 1927 , vol. 49, p. 250
106-39-8
4-溴氯苯
+
81745-84-8
→
反应条件
40133-23-1
2-(4-氯苯基)噻吩
反应条件
palladium; triphenylphosphine in tetrahydrofuran T=70°C; Negishi Coupling; 24 h; Inert atmosphereGreen chemistry; Catalytic behavior;
参考文献
Wu, Wei-Yi; Lin, Tze-Chiao; Takahashi, Tamotsu; Tsai, Fu-Yu; Mou, Chung-Yuan
ChemCatChem, 2013 , vol. 5, # 4 p. 1011 - 1019
649569-53-9
→
反应条件
40133-23-1
2-(4-氯苯基)噻吩
反应条件
1: With sulfuric acid in methanol 1 h; Heating; 2: With chloranil in benzene 2 h; Heating;
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
108-90-7
氯苯
→
反应条件
40133-23-1
2-(4-氯苯基)噻吩
反应条件
1.1: AlCl3 / CS2 / 2.5 h / 20 °C 2.1: dimethylformamide / 22 h / 5 °C 3.1: H2SO4 / methanol / 1 h / Heating 3.2: chloranil / benzene / 2 h / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
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