乙酯4-甲氧基苯并基甲酸盐合成路线 （共 31 条）
反应条件
in tetrahydrofuran T=-78°C; 1 h; Inert atmosphere;
参考文献
Infante, Rebeca; Nieto, Javier; Andres, Celia
Chemistry - A European Journal, 2012 , vol. 18, # 14 p. 4375 - 4379
反应条件
aluminium trichloride in dichloromethane T=20°C; Friedel-Crafts acylation; 1 h;
参考文献
Ianni, Alen; Waldvogel, Siegfried R.
Synthesis, 2006 , # 13 p. 2103 - 2112
反应条件
1: 1-bromo-4-methoxy-benzene With magnesium in tetrahydrofuran T=20°C; 1 h; Inert atmosphere; 2: oxalic acid diethyl ester in tetrahydrofuran T=-78°C; 2 h; Inert atmosphere;
参考文献
Hayashi, Masashi; Nakamura, Shuichi
Angewandte Chemie - International Edition, 2011 , vol. 50, # 10 p. 2249 - 2252
反应条件
boric acid; [Rh(OH)(cycloocta-1,5-diene)]2 in 1,4-dioxane T=60°C; 3 h;
参考文献
Shimizu, Hiroshi; Murakami, Masahiro
Chemical Communications, 2007 , # 27 p. 2855 - 2857
反应条件
bisacenaphthalenethiophene; oxygen in dichloromethane T=-78°C; 0.5 h; Irradiation;
参考文献
Wasserman, Harry H.; Ives, Jeffrey L.
Journal of Organic Chemistry, 1985 , vol. 50, # 19 p. 3573 - 3580
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 0.5 h;
参考文献
Katakura; Nagahara; Hara; Kunitada; Iwamoto
European Journal of Medicinal Chemistry, 1995 , vol. 30, # 5 p. 387 - 394
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-78 - 20°C;
参考文献
Thasana, Nopporn; Prachyawarakorn, Vilailak; Tontoolarug, Sopchok; Ruchirawat, Somsak
Tetrahedron Letters, 2003 , vol. 44, # 5 p. 1019 - 1021
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; calcium methanolate in acetonitrile T=0 - 20°C;
参考文献
Reddy, Sabbasani Rajasekhara; Stella, Selvaraj; Chadha, Anju
Synthetic Communications, 2012 , vol. 42, # 23 p. 3493 - 3503
反应条件
1: With (DHQD)2PHAL; methanesulfonamide; α-AD mix {K4[Fe(CN)6], OsO4, Na2CO3, (DHQ)2-PHAL} in water; tert-butyl alcohol T=0°C; Oxidation; Sharpless asymmetric dihydroxylation; 2: With water; sodium sulfite in tert-butyl alcohol T=0 - 20°C; Reduction; 0.75 h; Title compound not separated from byproducts;
参考文献
Monenschein, Holger; Draeger, Gerald; Jung, Alexander; Kirschning, Andreas
Chemistry - A European Journal, 1999 , vol. 5, # 8 p. 2270 - 2280
反应条件
2-hydroxy-1,3-isoindolinedione; oxygen; anhydrous cobalt diacetate in acetic acid T=40°C; Oxidation; 24 h;
参考文献
Wentzel, Bastienne B; Donners, Maurice P.J; Alsters, Paul L; Feiters, Martinus C; Nolte, Roeland J.M
Tetrahedron, 2000 , vol. 56, # 39 p. 7797 - 7803
