1: With isopropylmagnesium chloride in tetrahydrofuran
T=-20°C; 0.666667 h;
2: With lithium tetrachloromanganate(II); air in tetrahydrofuran
T=-20°C; 1 h; Further stages.;
参考文献
Cahiez, Gerard; Moyeux, Alban; Buendia, Julien; Duplais, Christophe
Journal of the American Chemical Society, 2007 , vol. 129, # 45 p. 13788 - 13789
Mishra, Sourabh; De, Subhadip; N Kakde, Badrinath; Dey, Dhananjay; Bisai, Alakesh
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2013 , vol. 52, # 8-9 p. 1093 - 1102
4-(N,N-dimethlyamino)pyridine; trifluoromethylsulfonic anhydride in dichloromethane
参考文献
Banwell, Martin G.; Bissett, Brett D.; Busato, Stefan; Cowden, Cameron J.; Hockless, David C. R.; et al.
Journal of the Chemical Society, Chemical Communications, 1995 , # 24 p. 2551 - 2554
tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide
24 h; electrochemical reduction;
参考文献
Grimshaw, James; Hamilton, Robert; Trocha-Grimshaw, Jadwiga
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 229 - 234