alpha-甲基-4-(2-甲基丙基)-苯甲醇合成路线 （共 24 条）
反应条件
sulfuric acid; dihydrogen peroxide; sodium tungstate in water; acetonitrile T=80°C; 6 h;
参考文献
Bhati, Nishi; Sarma, Kuladip; Goswami, Amrit
Synthetic Communications, 2008 , vol. 38, # 9 p. 1416 - 1424
反应条件
oxygen; (-)-sparteine; palladium diacetate in toluene T=80°C; P=760 Torr; Title compound not separated from byproducts;
参考文献
Thakur, Vinay V.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 3 p. 557 - 562
反应条件
1: With oxygen; (-)-sparteine; palladium diacetate in toluene T=80°C; P=760 Torr; 2: With pyridine; phosphorus tribromide in diethyl ether T=-20 - 0°C; Title compound not separated from byproducts;
参考文献
Thakur, Vinay V.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 3 p. 557 - 562
反应条件
1: 1-(4-isobutylphenyl)-ethanol With oxygen; (-)-sparteine; palladium diacetate in toluene T=80°C; P=760 Torr; 2: With pyridine; phosphorus tribromide in diethyl ether T=-20 - 0°C; 3: sodium cyanide in N,N-dimethyl-formamide T=80°C; Title compound not separated from byproducts;
参考文献
Thakur, Vinay V.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 3 p. 557 - 562
反应条件
Multistep reaction. Title compound not separated from byproducts;
参考文献
Thakur, Vinay V.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 3 p. 557 - 562
反应条件
Multistep reaction. Title compound not separated from byproducts;
参考文献
Thakur, Vinay V.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 3 p. 557 - 562
反应条件
Multistep reaction. Title compound not separated from byproducts;
参考文献
Thakur, Vinay V.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 3 p. 557 - 562
反应条件
toluene-4-sulfonic acid; triphenylphosphine; lithium chloride; palladium in water; butanone T=115°C; Carbonylation; P=40503.2 Torr; 8 h; Title compound not separated from byproducts;
参考文献
Sarkar, Bibhas R.; Chaudhari, Raghunath V.
Catalysis Today, 2012 , vol. 198, # 1 p. 154 - 173
反应条件
water; toluene-4-sulfonic acid; triphenylphosphine; lithium chloride; 1 Ni/ZSM 5 in butanone T=115°C; P=41372.9 Torr;
参考文献
Council of Scientific and Industrial Research
Patent: US6660883 B1, 2003 ;
Location in patent: Page column 52-54 ;
反应条件
toluene-4-sulfonic acid; triphenylphosphine; lithium chloride; palladium in water; butanone T=115°C; Carbonylation; P=40503.2 Torr; 8 h; Title compound not separated from byproducts;
参考文献
Sarkar, Bibhas R.; Chaudhari, Raghunath V.
Catalysis Today, 2012 , vol. 198, # 1 p. 154 - 173
