1,3-二乙基-2-甲氧基-5-硝基苯合成路线 (共 3 条)
反应条件
nitric acid in chloroform
T=25 - 30°C;
参考文献
Duffy; Dearden; Rostron
Journal of Pharmacy and Pharmacology, 2001 , vol. 53, # 11 p. 1505 - 1514
反应条件
1.1: aqueous sulfuric acid; sodium nitrite / 5 °C
1.2: 1 h / 50 °C
2.1: sodium ethoxide / ethanol / 3 h / Heating
3.1: nitric acid (70 percent) / CHCl3 / 25 - 30 °C
View Scheme
参考文献
Duffy; Dearden; Rostron
Journal of Pharmacy and Pharmacology, 2001 , vol. 53, # 11 p. 1505 - 1514
反应条件
1: sodium ethoxide / ethanol / 3 h / Heating
2: nitric acid (70 percent) / CHCl3 / 25 - 30 °C
View Scheme
参考文献
Duffy; Dearden; Rostron
Journal of Pharmacy and Pharmacology, 2001 , vol. 53, # 11 p. 1505 - 1514