1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C
1.2: 0.06 h / -78 - 20 °C
2.1: dichloromethane / 1 h / 20 °C
2.2: 6 h / 20 °C
3.1: [Ru(2,2′-bipyridine)3][hexafluorophosphate]2; hydroxybenziodoxole; sodium carbonate / dichloromethane; water / 12 h
View Scheme
参考文献
Huang, Hanchu; Zhang, Guojin; Gong, Li; Zhang, Shuaiyan; Chen, Yiyun
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2280 - 2283
1.1: dichloromethane / 1 h / 20 °C
1.2: 6 h / 20 °C
2.1: [Ru(2,2′-bipyridine)3][hexafluorophosphate]2; hydroxybenziodoxole; sodium carbonate / dichloromethane; water / 12 h
View Scheme
参考文献
Huang, Hanchu; Zhang, Guojin; Gong, Li; Zhang, Shuaiyan; Chen, Yiyun
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2280 - 2283
