3-chloro-benzenecarboperoxoic acid in dichloromethane
T=0°C; 0.5 h;
参考文献
Merricks, David; Sammes, Peter G.; Walker, Edward R. H.; Henrick, Kim; McPartlin, Mary M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , p. 2169 - 2176
1: 1) chlorine, 2) N(Et)3 / 1) CH2Cl2, 0 deg C, 10 min, 2) CH2Cl2, r. t., 1 h
2: 76 percent / 3-chloroperbenzoic acid / CH2Cl2 / 0.5 h / 0 °C
View Scheme
参考文献
Merricks, David; Sammes, Peter G.; Walker, Edward R. H.; Henrick, Kim; McPartlin, Mary M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , p. 2169 - 2176
1: 1) chlorine, 2) N(Et)3 / 1) CH2Cl2, 0 deg C, 10 min, 2) CH2Cl2, r. t., 1 h
2: 76 percent / 3-chloroperbenzoic acid / CH2Cl2 / 0.5 h / 0 °C
View Scheme
参考文献
Merricks, David; Sammes, Peter G.; Walker, Edward R. H.; Henrick, Kim; McPartlin, Mary M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , p. 2169 - 2176