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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
401792-87-8
合成路线
（共 10 条）
67-56-1
甲醇
+
201230-82-2
+
95652-81-6
6-氯-2-甲氧基-吡啶-3-甲醛
→
反应条件
401792-87-8
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; sodium acetate; palladium diacetate in toluene T=50°C; 23 h;
参考文献
Ouchi, Hitoshi; Asahina, Aya; Asakawa, Tomohiro; Inai, Makoto; Hamashima, Yoshitaka; Kan, Toshiyuki
Organic Letters, 2014 , vol. 16, # 7 p. 1980 - 1983
401792-84-5
→
反应条件
401792-87-8
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in water; acetic acid 1 h; Heating;
参考文献
Adamczyk, Maciej; Akireddy, Srinivasa Rao; Reddy, Rajarathnam E
Tetrahedron, 2002 , vol. 58, # 34 p. 6951 - 6963
2402-78-0
2,6-二氯吡啶
→
反应条件
401792-87-8
反应条件
1.1: methanol / 24 h / 60 °C 2.1: tert.-butyl lithium / tetrahydrofuran; n-heptane / 1 h / -78 °C / |Inert atmosphere 2.2: 1 h / -78 - 20 °C / |Inert atmosphere 3.1: sodium acetate; palladium diacetate; 1,1'-bis-(diphenylphosphino)ferrocene / toluene / 23 h / 50 °C View Scheme
参考文献
Ouchi, Hitoshi; Asahina, Aya; Asakawa, Tomohiro; Inai, Makoto; Hamashima, Yoshitaka; Kan, Toshiyuki
Organic Letters, 2014 , vol. 16, # 7 p. 1980 - 1983
17228-64-7
2-氯-6-甲氧基吡啶
→
反应条件
401792-87-8
反应条件
1.1: tert.-butyl lithium / tetrahydrofuran; n-heptane / 1 h / -78 °C / |Inert atmosphere 1.2: 1 h / -78 - 20 °C / |Inert atmosphere 2.1: sodium acetate; palladium diacetate; 1,1'-bis-(diphenylphosphino)ferrocene / toluene / 23 h / 50 °C View Scheme
参考文献
Ouchi, Hitoshi; Asahina, Aya; Asakawa, Tomohiro; Inai, Makoto; Hamashima, Yoshitaka; Kan, Toshiyuki
Organic Letters, 2014 , vol. 16, # 7 p. 1980 - 1983
589-93-5
2,5-二甲基吡啶
→
反应条件
401792-87-8
反应条件
1.1: SeO2 / pyridine / 26 h / Heating 2.1: 8.2 g / conc. H2SO4 / 8 h / Heating 3.1: 78 percent / m-CPBA / CHCl3 / 15 h / 20 °C 4.1: Ac2O / 3 h / Heating 4.2: 51 percent / NaOMe / methanol / 0.17 h / 0 °C 5.1: 93 percent / Ag2CO3 / CHCl3 / 120 h / 20 °C 6.1: 77 percent / AIBN; NBS / CCl4 / Heating 7.1: 34 percent / hexamethylenetetramine; aq. acetic acid / 1 h / Heating View Scheme
参考文献
Adamczyk, Maciej; Akireddy, Srinivasa Rao; Reddy, Rajarathnam E
Tetrahedron, 2002 , vol. 58, # 34 p. 6951 - 6963
29681-38-7
5-甲基吡啶-2-羧酸甲酯
→
反应条件
401792-87-8
反应条件
1.1: 78 percent / m-CPBA / CHCl3 / 15 h / 20 °C 2.1: Ac2O / 3 h / Heating 2.2: 51 percent / NaOMe / methanol / 0.17 h / 0 °C 3.1: 93 percent / Ag2CO3 / CHCl3 / 120 h / 20 °C 4.1: 77 percent / AIBN; NBS / CCl4 / Heating 5.1: 34 percent / hexamethylenetetramine; aq. acetic acid / 1 h / Heating View Scheme
参考文献
Adamczyk, Maciej; Akireddy, Srinivasa Rao; Reddy, Rajarathnam E
Tetrahedron, 2002 , vol. 58, # 34 p. 6951 - 6963
401792-77-6
5-甲基-2-吡啶羧酸甲酯 N-氧化物
→
反应条件
401792-87-8
反应条件
1.1: Ac2O / 3 h / Heating 1.2: 51 percent / NaOMe / methanol / 0.17 h / 0 °C 2.1: 93 percent / Ag2CO3 / CHCl3 / 120 h / 20 °C 3.1: 77 percent / AIBN; NBS / CCl4 / Heating 4.1: 34 percent / hexamethylenetetramine; aq. acetic acid / 1 h / Heating View Scheme
参考文献
Adamczyk, Maciej; Akireddy, Srinivasa Rao; Reddy, Rajarathnam E
Tetrahedron, 2002 , vol. 58, # 34 p. 6951 - 6963
401792-80-1
甲基5-甲基-6-氧代-1,6-二氢-2-吡啶羧酸酯
→
反应条件
401792-87-8
反应条件
1: 93 percent / Ag2CO3 / CHCl3 / 120 h / 20 °C 2: 77 percent / AIBN; NBS / CCl4 / Heating 3: 34 percent / hexamethylenetetramine; aq. acetic acid / 1 h / Heating View Scheme
参考文献
Adamczyk, Maciej; Akireddy, Srinivasa Rao; Reddy, Rajarathnam E
Tetrahedron, 2002 , vol. 58, # 34 p. 6951 - 6963
401792-82-3
→
反应条件
401792-87-8
反应条件
1: 77 percent / AIBN; NBS / CCl4 / Heating 2: 34 percent / hexamethylenetetramine; aq. acetic acid / 1 h / Heating View Scheme
参考文献
Adamczyk, Maciej; Akireddy, Srinivasa Rao; Reddy, Rajarathnam E
Tetrahedron, 2002 , vol. 58, # 34 p. 6951 - 6963
4434-13-3
5-甲基-2-甲酸吡啶
→
反应条件
401792-87-8
反应条件
1.1: 8.2 g / conc. H2SO4 / 8 h / Heating 2.1: 78 percent / m-CPBA / CHCl3 / 15 h / 20 °C 3.1: Ac2O / 3 h / Heating 3.2: 51 percent / NaOMe / methanol / 0.17 h / 0 °C 4.1: 93 percent / Ag2CO3 / CHCl3 / 120 h / 20 °C 5.1: 77 percent / AIBN; NBS / CCl4 / Heating 6.1: 34 percent / hexamethylenetetramine; aq. acetic acid / 1 h / Heating View Scheme
参考文献
Adamczyk, Maciej; Akireddy, Srinivasa Rao; Reddy, Rajarathnam E
Tetrahedron, 2002 , vol. 58, # 34 p. 6951 - 6963
