1: With sodium hydrogencarbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide T=150°C; Heck reaction; 20 h; 2: With hydrogenchloride in tetrahydrofuran T=25°C; Further stages.;
参考文献
Battace, Ahmed; Feuerstein, Marie; Lemhadri, Mhamed; Zair, Touriya; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2007 , # 19 p. 3122 - 3132
1: 1-trifluoromethyl-4-bromobenzene With magnesium in tetrahydrofuran T=20°C; Inert atmosphere; 2: N-methoxy-N-methylpropionamide in tetrahydrofuran T=-20 - 20°C; Inert atmosphere; 3: With water in tetrahydrofuran
参考文献
Ueno, Satoshi; Shimizu, Ryosuke; Kuwano, Ryoichi
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 4543 - 4545
Angewandte Chemie, 2009 , vol. 121, p. 4613 - 4615
