sodium carbonate; potassium iodide in N,N-dimethyl-formamide T=80°C; 24 h;

1: 1-phenyl-piperazine; JandaJel-REM in N,N-dimethyl-formamide T=20°C; Solid phase reaction; Michael addition; 24 h; 2: 1-bromomethyl-4-nitro-benzene in N,N-dimethyl-formamide T=20°C; Solid phase reaction; alkylation; 24 h; 3: With NCPS-NEt2 in dichloromethane T=20°C; Solid phase reaction; elimination; 24 h; Further stages.;

hydrogen; PtO2 in methanol; acetonitrile

triethylamine

暂无反应条件数据