3-甲基苯基(三甲基硅)乙炔合成路线 （共 6 条）
反应条件
water; triethylamine; triphenylphosphine; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in tetrahydrofuran T=160°C; P=51485.6 Torr; 4 h;
参考文献
Takeuchi, Ryo; Yasue, Hiroyuki
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5386 - 5392
反应条件
potassium carbonate in methanol T=25°C; 3 h;
参考文献
Wang, Yue; Huang, Bin; Sheng, Shouri; Cai, Mingzhong
Journal of Chemical Research, 2007 , # 12 p. 728 - 732
反应条件
1: potassium carbonate / methanol / 7 h / 20 °C 2: tetrakis(triphenylphosphine) palladium(0); hydrogenchloride / tetrahydrofuran; water / 168 h / 45 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Xu, Caixia; Du, Weiyuan; Zeng, Yi; Dai, Bin; Guo, Hao
Organic Letters, 2014 , vol. 16, # 3 p. 948 - 951
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine in toluene
T=20°C; 3 h; Inert atmosphereSchlenk technique;
参考文献
Xu, Caixia; Du, Weiyuan; Zeng, Yi; Dai, Bin; Guo, Hao
Organic Letters, 2014 , vol. 16, # 3 p. 948 - 951
反应条件
copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0)
Heating;
参考文献
Musso, David L; Clarke, Morris J; Kelley, James L; Boswell, G Evan; Chen, Grace
Organic and biomolecular chemistry, 2003 , vol. 1, # 3 p. 498 - 506
反应条件
palladium
Sonogashira coupling;
参考文献
Atienza; Mateo; de Frutos; Echavarren
Organic letters, 2001 , vol. 3, # 2 p. 153 - 155
