3,5-二甲基-1H-吡咯-2-甲酸苄酯合成路线 （共 13 条）
反应条件
1: 90 percent / glacial acetic acid; HCl / H2O / 3 h / 40 °C
2: Et3N; H2 / Pd/C / tetrahydrofuran / 20 h / 20 °C
View Scheme
参考文献
Thompson; Dolphin
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7870 - 7877
反应条件
1.1: titanium tetrachloride / dichloromethane / 2 h / 0 °C / |Inert atmosphere
2.1: borane-THF / tetrahydrofuran / 1 h / 0 °C / |Inert atmosphere
2.2: 0.5 h / 0 °C
View Scheme
参考文献
Lundrigan, Travis; Jackson, Carla L. M.; Uddin, Md. Imam; Tucker, Lloyd A.; Cameron, T. Stanley; Thompson, Alison; Ali, Adeeb Al-Sheikh; Linden, Anthony
Canadian Journal of Chemistry, 2012 , vol. 90, # 8 p. 693 - 700,8
反应条件
1: SnCl4 / CH2Cl2; nitromethane
2: NaBH4
3: sulphonyl chloride
4: H2O
5: hydrogen / Pd/C
View Scheme
参考文献
Nishide, Hiroyuki; Hashimoto, Yukio; Maeda, Hiromi; Tsuchida, Eishun
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1987 , p. 2963 - 2968
