cerium(III) chloride in tetrahydrofuran T=20°C;

1: 76 percent / anhydrous cerium(III) chloride / tetrahydrofuran / 20 °C 2: 50 percent / potassium hydrogen sulfate / 3 h / 110 °C / 180.01 Torr View Scheme

1.1: 76 percent / anhydrous cerium(III) chloride / tetrahydrofuran / 20 °C 2.1: 50 percent / potassium hydrogen sulfate / 3 h / 110 °C / 180.01 Torr 3.1: methyl magnesium chloride / tetrahydrofuran / 2 h / Heating 3.2: 80 percent / tetrahydrofuran / Heating View Scheme

1.1: 76 percent / anhydrous cerium(III) chloride / tetrahydrofuran / 20 °C 2.1: 50 percent / potassium hydrogen sulfate / 3 h / 110 °C / 180.01 Torr 3.1: methyl magnesium chloride / tetrahydrofuran / 2 h / Heating 3.2: 80 percent / tetrahydrofuran / Heating 4.1: 83 percent / lithium aluminum hydride / tetrahydrofuran / 3 h / Heating View Scheme