4-硝基-α-甲苯磺酰氯合成路线 （共 21 条）
反应条件
hydrogenchloride; sodium chlorite in acetonitrile T=10 - 20°C; 0.5 h; Green chemistry;
参考文献
Yang, Zhanhui; Zheng, Yongpeng; Xu, Jiaxi
Synlett, 2013 , vol. 24, # 16 art. no. ST-2013-W0601-L, p. 2165 - 2169
反应条件
phosphorus pentachloride
参考文献
Auspex Pharmaceuticals, Inc.
Patent: US2008/103189 A1, 2008 ;
Location in patent: Page/Page column 38 ;
反应条件
hydrogenchloride; N-chloro-succinimide in acetonitrile T=10°C;
参考文献
Nishiguchi, Atsuko; Maeda, Kazuhiro; Miki, Shokyo
Synthesis, 2006 , # 24 p. 4131 - 4134
反应条件
in chloroform; water; toluene
参考文献
Fabre-Kramer Pharmaceuticals, Inc.
Patent: US2009/281114 A1, 2009 ;
US 20090281114 A1
参考文献
Lee, Ikchoon; Kang, Han Keun; Lee, Hai Whang
Journal of the American Chemical Society, 1987 , vol. 109, # 24 p. 7472 - 7477
反应条件
1: sodium sulfite View Scheme
参考文献
Yang, Zhanhui; Zheng, Yongpeng; Xu, Jiaxi
Synlett, 2013 , vol. 24, # 16 art. no. ST-2013-W0601-L, p. 2165 - 2169
反应条件
phosphorus pentachloride; trichlorophosphate T=90°C;
参考文献
Ingold; Ingold; Shaw
Journal of the Chemical Society, 1927 , p. 818
参考文献
Rohm and Haas Co.
Patent: US2174856 , 1938 ;
反应条件
propan-1-ol; tetrachloromethane; chlorine
参考文献
Baganz; Kessler
Chemische Berichte, 1955 , vol. 88, p. 1995
反应条件
1: nitric acid 2: phosphoryl chloride; phosphorus pentachloride / 90 °C View Scheme
参考文献
Ingold; Ingold; Shaw
Journal of the Chemical Society, 1927 , p. 818
