反应条件
1: 1.) 1,3-dicyclohexylcarbodiimide, CuCl / 1.) 60 deg C, 6 h, 2.) C6H6, reflux, 24 h 2: 45 percent / KF, Kryptofix 222 / dimethylsulfoxide / 24 h / 160 °C 3: 61 percent / aq. HBr / acetic acid / 3 h / Ambient temperature 4: 71 percent / triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 90 h / Ambient temperature 5: 74 percent / CF3COOH / CH2Cl2 / 3 h / Ambient temperature View Scheme
参考文献
Horti, Andrew G.; Koren, Andrei O.; Ravert, Hayden T.; Musachio, John L.; Mathews, William B.; London, Edythe D.; Dannals, Robert F.
Journal of Labelled Compounds and Radiopharmaceuticals, 1998 , vol. 41, # 4 p. 309 - 318
