(E)-N,N-二乙基-3,7-二甲基-2,6-辛二烯-1-胺合成路线 （共 10 条）
反应条件
1: 92 percent / 50percent sulfuric acid / H2O / 1 h / 0 °C 2: 93.5 percent Chromat. / <Pd(η3-C3H5)Ph2p(CH2)5PPh2>(+)ClO4(-) / 3 h / 130 °C / 20 Torr / other catalysts 3: 92 percent View Scheme
参考文献
Kumobayashi, Hidenori; Mitsuhashi, Shigeru; Akutagawa, Susumu; Ohtsuka, Sei
Chemistry Letters, 1986 , p. 157 - 160
反应条件
tert.-butylhydroperoxide in 2,2,4-trimethylpentane; dichloromethane
参考文献
Rhone-Poulenc Nutrition Animale
Patent: US5202497 A1, 1993 ;
反应条件
bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate; polymer-anchored (R)-BINAP in tetrahydrofuran 20 h; Heating;
参考文献
Chapuis, Christian; Barthe, Michel; Laumer, Jean-Yves de Saint
Helvetica Chimica Acta, 2001 , vol. 84, # 1 p. 230 - 242
反应条件
lt;Pd(η-C3H5)Ph2p(CH2)4PPhgt;(2+)*ClO4(1-) T=130°C; P=20 Torr; 5 h;
参考文献
Kumobayashi, Hidenori; Mitsuhashi, Shigeru; Akutagawa, Susumu; Ohtsuka, Sei
Chemistry Letters, 1986 , p. 157 - 160
反应条件
(S)-6,6'-bis(Ph2P)-2'-[(TentaGel S-yl)oxy] [1,1'biPh]-2-ol; bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate in tetrahydrofuran 20 h; Heating; Product distribution; Further Variations:CatalystsReagents;
参考文献
Chapuis, Christian; Barthe, Michel; Laumer, Jean-Yves de Saint
Helvetica Chimica Acta, 2001 , vol. 84, # 1 p. 230 - 242
反应条件
lt;Pd(η-C3H5)Ph2p(CH2)2Phgt;(2+)*ClO4(1-) T=130°C; P=20 Torr; 3 h;
参考文献
Chemistry Letters, , p. 157 - 160
反应条件
1: 92 percent / 50percent sulfuric acid / H2O / 1 h / 0 °C
2: 1.5 percent Chromat. / <Pd(η3-C3H5)Ph2p(CH2)5PPh2>(+)ClO4(-) / 3 h / 130 °C / 20 Torr / other catalysts
View Scheme
参考文献
Kumobayashi, Hidenori; Mitsuhashi, Shigeru; Akutagawa, Susumu; Ohtsuka, Sei
Chemistry Letters, 1986 , p. 157 - 160
反应条件
lt;Pd(η-C3H5)Ph2p(CH2)2Phgt;(2+)*ClO4(1-)
T=130°C; P=20 Torr; 3 h;
参考文献
Kumobayashi, Hidenori; Mitsuhashi, Shigeru; Akutagawa, Susumu; Ohtsuka, Sei
Chemistry Letters, 1986 , p. 157 - 160
反应条件
1: 92 percent / 50percent sulfuric acid / H2O / 1 h / 0 °C
2: 93.5 percent Chromat. / <Pd(η3-C3H5)Ph2p(CH2)5PPh2>(+)ClO4(-) / 3 h / 130 °C / 20 Torr / other catalysts
View Scheme
参考文献
Kumobayashi, Hidenori; Mitsuhashi, Shigeru; Akutagawa, Susumu; Ohtsuka, Sei
Chemistry Letters, 1986 , p. 157 - 160
反应条件
lt;Pd(η-C3H5)Ph2p(CH2)2Phgt;(2+)*ClO4(1-)
T=130°C; P=20 Torr; 3 h;
参考文献
Kumobayashi, Hidenori; Mitsuhashi, Shigeru; Akutagawa, Susumu; Ohtsuka, Sei
Chemistry Letters, 1986 , p. 157 - 160
