2,5-二甲氧基-β-硝基苯乙烯合成路线 （共 6 条）
反应条件
potassium hydroxide; ethanol Behandeln des Reaktionsproduktes mit Salzsaeure;
参考文献
Solomonovici,A.; Blumberg,S.
Tetrahedron, 1966 , vol. 22, p. 2505 - 2509
参考文献
Kauffmann
Chemische Berichte, 1917 , vol. 50, p. 635
Chemische Berichte, 1919 , vol. 52, p. 1431
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Heating;
参考文献
Cheng; Castagnoli Jr.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 4 p. 513 - 520
反应条件
1: 76 percent / LiAlH4 / tetrahydrofuran / Heating 2: BBr3 / CH2Cl2 / 48 h / Ambient temperature View Scheme
参考文献
Cromartie; Harley-Mason
Journal of the Chemical Society, 1952 , p. 2525
反应条件
1: 76 percent / LiAlH4 / tetrahydrofuran / Heating
2: 80 percent / acetic acid, nitric acid / 1 h / 0 °C
View Scheme
参考文献
Cheng; Castagnoli Jr.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 4 p. 513 - 520
反应条件
1: 76 percent / LiAlH4 / tetrahydrofuran / Heating
2: 80 percent / acetic acid, nitric acid / 1 h / 0 °C
3: 48 percent / concd HCl, Sn / 1 h / Heating
View Scheme
参考文献
Cheng; Castagnoli Jr.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 4 p. 513 - 520
