苄氧羰基-亮氨酰-丝氨酸甲酯合成路线 (共 4 条)
反应条件
4-methyl-morpholine; thylchlorophormate in ethyl acetate
-15 deg C, 1 h, then RT, 12 h;
参考文献
Falorni; Giacomelli; Satta; Cossu
Synthesis, 1994 , # 4 p. 391 - 395
反应条件
4-methyl-morpholine in ethyl acetate
T=-15 - 20°C; 13 h; Yield given;
参考文献
Falorni, Massimo; Satta, Michele; Conti, Sandra; Giacomelli, Giampaolo
Tetrahedron: Asymmetry, 1993 , vol. 4, # 11 p. 2389 - 2398
反应条件
1: 4-methylmorpholine / ethyl acetate / 0.25 h / -15 °C
2: 4-methylmorpholine / ethyl acetate / 13 h / -15 - 20 °C
View Scheme
参考文献
Falorni, Massimo; Satta, Michele; Conti, Sandra; Giacomelli, Giampaolo
Tetrahedron: Asymmetry, 1993 , vol. 4, # 11 p. 2389 - 2398
反应条件
(i) Et3N, dimethoxyethane, (ii) N,N-dimethyl-propanediyl-diamine; Multistep reaction;
参考文献
Schattenkerk,C. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1973 , vol. 92, p. 92 - 116