(4-溴苯基)(4-硝基苯基)甲酮合成路线 （共 12 条）
反应条件
AlCl3, aluminium chloride
参考文献
ALLERGAN, INC.
Patent: WO2008/22013 A1, 2008 ;
Location in patent: Page/Page column 15 ;
WO 2008/022013 A1
反应条件
1: With Chromium (III) chloride in various solvent(s) T=20°C; Addition; 8 h; 2: With benzaldehyde in various solvent(s) T=20°C; Oxidation; Further stages.;
参考文献
Ogawa, Yoshihiro; Saiga, Akihiro; Mori, Mitsuo; Shibata, Takanori; Takagi, Kentaro
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 1031 - 1036
反应条件
aluminium trichloride T=75 - 85°C;
参考文献
Allergan, Inc.
Patent: US2007/32478 A1, 2007 ;
Location in patent: Page/Page column 69 ;
US 20070032478 A1
反应条件
potassium acetate; sodium hydrogencarbonate; iron(II) chloride T=100°C; Suzuki Coupling; P=760.051 Torr; 12 h; Schlenk technique;
参考文献
Zhong, Yanzhen; Han, Wei
Chemical Communications, 2014 , vol. 50, # 29 p. 3874 - 3877
反应条件
1: With KF*2H2O; copper(II) bis(trifluoromethanesulfonate); 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene T=-20 - 20°C; 6 h; Inert atmosphere; 2: With oxygen in toluene T=20 - 120°C; 24.5 h;
参考文献
Zheng, Hanmei; Ding, Jinchang; Chen, Jiuxi; Liu, Miaochang; Gao, Wenxia; Wu, Huayue
Synlett, 2011 , # 11 p. 1626 - 1630
反应条件
P2O5/silica gel Friedel Crafts acylation; 3 h; Reflux;
参考文献
Zarei, Amin; Hajipour, Abdol R.; Khazdooz, Leila
Tetrahedron Letters, 2008 , vol. 49, # 47 p. 6715 - 6719
反应条件
carbon disulfide; aluminium trichloride T=60°C; Oxydieren des Reaktionsproduktes mit CrO3 in Essigsaeure;
参考文献
Montagne
Chemische Berichte, 1916 , vol. 49, p. 2274
反应条件
carbon disulfide; aluminium trichloride T=60°C; Kochen des Reaktionsproduktes mit CrO3 in Essigsaeure;
参考文献
Montagne
Chemische Berichte, 1916 , vol. 49, p. 2274
反应条件
aluminum oxide; hexaoxo-.mu.-peroxodisulfate(2-); zirconium oxide T=150°C; Friedel-Crafts reaction; 4 h; Title compound not separated from byproducts;
参考文献
Jin, Tong-Shou; Yang, Mi-Na; Feng, Guo-Liang; Li, Tong-Shuang
Synthetic Communications, 2004 , vol. 34, # 3 p. 479 - 485
反应条件
1: AlCl3 2: CrO3 View Scheme
参考文献
Boeseken
Recueil des Travaux Chimiques des Pays-Bas, 1904 , vol. 23, p. 107
