1-(4-氟苯基)-1-乙醇合成路线 (共 81 条)
反应条件
[bis(acetoxy)iodo]benzene; potassium bromide; (S,S)-(+)-Jacobsen salene complex in dichloromethane T=20°C; 1 h; Kinetics; Further Variations:Solvents;
参考文献
Li, Zhen; Tang, Zhong H.; Hu, Xiao X.; Xia, Chun G.
Chemistry - A European Journal, 2005 , vol. 11, # 4 p. 1210 - 1216
反应条件
in acetone T=25°C; 3 h;
参考文献
Kovac, F.; Baumstark, A. L.
Tetrahedron Letters, 1994 , vol. 35, # 47 p. 8751 - 8754
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 24 h / 25 °C 2: iodine / neat (no solvent) / 2 h / 85 °C View Scheme
参考文献
Jereb, Marjan; Vrazic, Dejan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 12 p. 1978 - 1999
反应条件
[(Ph4Cp-OH)Ru(CO)2]2 in benzene-d6 T=70°C; Kinetics;
参考文献
Johnson, Jeffrey B.; Baeckvall, Jan-E.
Journal of Organic Chemistry, 2003 , vol. 68, # 20 p. 7681 - 7684
反应条件
[(Ph4Cp-OH)Ru(CO)2]2 in benzene-d6 T=70°C; Kinetics;
参考文献
Journal of Organic Chemistry, , vol. 68, # 20 p. 7681 - 7684
反应条件
phosphorus tribromide in dichloromethane T=4 - 20°C; 4 h;
参考文献
Gruenenthal GmbH
Patent: US2012/46301 A1, 2012 ;
Location in patent: Page/Page column 30; 31 ;
US 20120046301 A1
反应条件
3 A molecular sieve; oxygen; (-)-sparteine; palladium dichloro (η-2,5-norbornadiene) in toluene T=80°C; P=760.051 Torr; 54 h;
参考文献
Journal of the American Chemical Society, , vol. 123, # 31 p. 7725 - 7726
反应条件
sodium isopropanolate; acetone; [RuCl2(PPh3)(ferrocenyloxazolinylphosphine)] in isopropyl alcohol T=50°C; 0.583333 h;
参考文献
Chen, Tao; Jiang, Jia-Jun; Xu, Qin; Shi, Min
Organic Letters, 2007 , vol. 9, # 5 p. 865 - 868
反应条件
(1S,2R)-(+)-erythro-2-amino-1,2-diphenylethanol; benzoic acid in hexane T=20°C; 12 h;
参考文献
Kodama, Koichi; Sekine, Eriko; Hirose, Takuji
Chemistry - A European Journal, 2011 , vol. 17, # 41 p. 11527 - 11534
反应条件
triethylamine; planar-chiral DMAP derivative in 1,1-dimethylpropan-1-ol T=0°C; Acetylation;
参考文献
Ruble, J. Craig; Tweddell, Jennifer; Fu, Gregory C.
Journal of Organic Chemistry, 1998 , vol. 63, # 9 p. 2794 - 2795