aluminium trichloride in dichloromethane T=15°C; 1 h;
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1: CH2Cl2 / 5 h / Ambient temperature 2: H2 / 10percent Pd-C / ethanol / 8 h / 100 °C View Scheme
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n-butyllithium in tetrahydrofuran; hexane T=-78°C; 16 h; Inert atmosphere;
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