1-环丙基-4-甲氧基苯合成路线 （共 29 条）
反应条件
1: lithium thiophenoxide; cyclopropyl-magnesium bromide in tetrahydrofuran
T=60°C; 1 h;
2: 2-methoxy 5-cyanobenzene With n-tridecane; [NiCl2(PMe3)2] in tetrahydrofuran
T=60°C; 15 h;
参考文献
Miller, Joseph A.; Dankwardt, John W.
Tetrahedron Letters, 2003 , vol. 44, # 9 p. 1907 - 1910
反应条件
5,10,15,20-tetrakisphenylporphyrinatoiron(III) chloride; potassium hydroxide in water
4 h;
参考文献
Morandi, Bill; Carreira, Erick M.
Science, 2012 , vol. 335, # 6075 p. 1471 - 1474
反应条件
1: Zn(CH2I)2 With ethylene glycol dimethyl ether; trichloroacetic acid in hexane; dichloromethane
T=-15°C; Simmons-Smith Cyclopropanation; 1 h; Schlenk techniqueInert atmosphere;
2: 4-methoxy-1-vinyl-benzene in hexane; dichloromethane
T=-15 - 25°C; Simmons-Smith Cyclopropanation; 18 h; Schlenk techniqueInert atmosphere;
参考文献
Cheng, Donghao; Huang, Deshun; Shi, Yian
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 34 p. 5588 - 5591
反应条件
PEPPSI Pd catalyst in tetrahydrofuran
T=65°C; Negishi coupling reaction; 4 h; Inert atmosphere;
参考文献
Coleridge, Brian M.; Bello, Charles S.; Leitner, Andreas
Tetrahedron Letters, 2009 , vol. 50, # 31 p. 4475 - 4477
反应条件
lithium aluminium tetrahydride in diethyl ether
168 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Oelschlager; Hellwich; Rothley
Archiv der Pharmazie, 1994 , vol. 327, # 4 p. 261 - 265
参考文献
Shono,T.; Nishiguchi,I.
Tetrahedron, 1974 , vol. 30, p. 2183 - 2190
反应条件
potassium hydroxide; fired clay; platinum
参考文献
Levina et al.
Vestnik Moskovskogo Universiteta, 1957 , vol. 12, # 5 p. 145
Chem.Abstr., 1959 , # 1194
反应条件
1: With lead(IV) acetate in acetic acid
T=70°C; Acetoxylation;
2: With lithium aluminium tetrahydride in tetrahydrofuran
Reduction; Heating;
参考文献
Riley; Hanzlik
Xenobiotica, 1994 , vol. 24, # 1 p. 1 - 16
反应条件
trifluoroacetic acid
T=20°C; 24 h; Yield given;
参考文献
Shabarov, Yu. S.; Saginova, L. G.; Veselovskaya, S. V.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, p. 685 - 689
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 4 p. 768 - 772
