2,5-二甲基-1-苯基-磷杂环戊烷合成路线 (共 4 条)
反应条件
(η5-Me5C5)2LaCH(Me3Si)2 in benzene-d6
T=-78 - 22°C;
参考文献
Douglass; Stern; Marks
Journal of the American Chemical Society, 2001 , vol. 123, # 42 p. 10221 - 10238
反应条件
1: 61 percent / tetrahydrofuran / 1.5 h
2: 20 percent / Li / tetrahydrofuran / 2.5 h
3: Cp'2LaCH(TMS)2 / benzene-d6 / -78 - 22 °C
View Scheme
参考文献
Douglass; Stern; Marks
Journal of the American Chemical Society, 2001 , vol. 123, # 42 p. 10221 - 10238
反应条件
1: 61 percent / tetrahydrofuran / 1.5 h
2: 20 percent / Li / tetrahydrofuran / 2.5 h
3: Cp'2LaCH(TMS)2 / benzene-d6 / -78 - 22 °C
View Scheme
参考文献
Douglass; Stern; Marks
Journal of the American Chemical Society, 2001 , vol. 123, # 42 p. 10221 - 10238
反应条件
1: 20 percent / Li / tetrahydrofuran / 2.5 h
2: Cp'2LaCH(TMS)2 / benzene-d6 / -78 - 22 °C
View Scheme
参考文献
Douglass; Stern; Marks
Journal of the American Chemical Society, 2001 , vol. 123, # 42 p. 10221 - 10238