己-4,5-二烯-1-醇合成路线 （共 12 条）
反应条件
La[N(TMS)2]3 in benzene-d6 T=130°C;
参考文献
Yu, Xianghua; Seo, SungYong; Marks, Tobin J.
Journal of the American Chemical Society, 2007 , vol. 129, # 23 p. 7244 - 7245
反应条件
(Me2Si(η5-Me4C5)(tBuN))Th(NMe2)2 in deuterated toluene T=120°C; Inert atmosphereGlovebox;
参考文献
Wobser, Stephen D.; Marks, Tobin J.
Organometallics, 2013 , vol. 32, # 9 p. 2517 - 2528
反应条件
diisopropylamine; copper(I) bromide in 1,4-dioxane
Crabbe reaction; 18 h; Heating;
参考文献
Grigg; MacLachlan; Rasparini
Chemical Communications, 2000 , # 22 p. 2241 - 2242
反应条件
hydrogenchloride in diethyl ether
18 h; Ambient temperature;
参考文献
Coates, Robert M.; Senter, Peter D.; Baker, William R.
Journal of Organic Chemistry, 1982 , vol. 47, # 19 p. 3597 - 3607
反应条件
BF3·2HOAc in dichloromethane
-10 degC, 5 min, 20 degC, 1.5 h;
参考文献
Pornet, J.; Damour, D.; Miginiac, L.
Journal of Organometallic Chemistry, 1987 , vol. 319, p. 333 - 344
反应条件
BF3·2HOAc in dichloromethane
-10 degC, 5 min, 20 degC, 1.5 h;
参考文献
Pornet, J.; Damour, D.; Miginiac, L.
Journal of Organometallic Chemistry, 1987 , vol. 319, p. 333 - 344
反应条件
copper(l) iodide; N-ethyl-N,N-diisopropylamine in 1,4-dioxane
18 h; Heating;
参考文献
Bates, Roderick W.; Rama-Devi, Thota; Ko, Huei-Huei
Tetrahedron, 1995 , vol. 51, # 47 p. 12939 - 12954
反应条件
in dichloromethane
-10 degC, 5 min, 20 degC, 1.5 h;
参考文献
Pornet, J.; Damour, D.; Miginiac, L.
Journal of Organometallic Chemistry, 1987 , vol. 319, p. 333 - 344
反应条件
toluene-4-sulfonic acid in methanol
参考文献
Arseniyadis,S. et al.
Tetrahedron, 1979 , vol. 35, p. 353 - 363
反应条件
hydrogenchloride; methyllithium
1) Et2O, -50 to 20 degC, 2) 20 degC; Yield given;
参考文献
Baker, William R.; Senter, Peter D.; Coates, Robert M.
Journal of the Chemical Society, Chemical Communications, 1980 , # 21 p. 1011 - 1012
