2,5-二甲氧基二苯甲酮合成路线 （共 27 条）
反应条件
aluminium trichloride in benzene T=80°C; 12 h;
参考文献
Sharghi, Hashem; Tamaddon, Fatemeh
Tetrahedron, 1996 , vol. 52, # 43 p. 13623 - 13640
参考文献
Bogert; Howells
Journal of the American Chemical Society, 1930 , vol. 52, p. 837,844
反应条件
tin(IV) chloride in benzene
Heating;
参考文献
Crescente, Oscar; Heller, Harry G.; Patharakorn, Surapol
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1599 - 1602
反应条件
1: With dimethyl sulfoxide; trifluoroacetic acid; palladium diacetate
T=100°C; 24 h;
2: With water
T=70°C; 2 h;
参考文献
Zhou, Chengxiang; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 9 p. 3551 - 3558
反应条件
carbon in benzene
T=20°C; 8 h; Heating / reflux;
参考文献
MERCK and CO., INC.; MERCK FROSST CANADA LTD.
Patent: WO2006/98912 A1, 2006 ;
Location in patent: Page/Page column 48-49 ;
WO 2006/098912 A1
反应条件
bismuth trifluoromethanesulphonate
Friedel-Crafts acylation; 0.0833333 h; Ionic liquidMicrowave irradiation;
参考文献
Tran, Phuong Hoang; Duus, Fritz; Le, Thach Ngoc
Tetrahedron Letters, 2012 , vol. 53, # 2 p. 222 - 224
反应条件
[2,2']bipyridinyl; Fe/Cr/Ni in N,N-dimethyl-formamide
Nozaki-Hiyama-Kishi reaction; Electrolysis;
参考文献
Durandetti; Nedelec; Perichon
Organic letters, 2001 , vol. 3, # 13 p. 2073 - 2076
反应条件
methanesulfonic acid; phosphorus pentoxide
T=60°C; Acylation; 2 h;
参考文献
Yonezawa, Noriyuki; Hino, Tetsuo; Matsuda, Kazuhisa; Matsuki, Toshiyuki; Narushima, Daisuke; Kobayashi, Masato; Ikeda, Tomiki
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 941 - 944
反应条件
carbon disulfide; aluminium trichloride
und Erwaermen des nach der Hydrolyse erhaltenen Reaktionsprodukts mit AlCl3 in Benzol;
参考文献
Bogert; Howells
Journal of the American Chemical Society, 1930 , vol. 52, p. 837,844
反应条件
trifluoromethanesulfonic acid 2-pyridinyl ester; trifluoroacetic acid
5 h; Heating;
参考文献
Keumi, Takashi; Yoshimura, Kiichiro; Shimada, Masakazu; Kitajima, Hidehiko
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 455 - 460
