3,4-二甲氧基二苯甲酮合成路线 （共 27 条）
反应条件
bismuth trifluoromethanesulphonate Friedel-Crafts acylation; 0.0833333 h; Ionic liquidMicrowave irradiation;
参考文献
Tran, Phuong Hoang; Duus, Fritz; Le, Thach Ngoc
Tetrahedron Letters, 2012 , vol. 53, # 2 p. 222 - 224
反应条件
silver perchlorate; niobium pentachloride in nitromethane T=80°C; Friedel-Crafts acylation; 7 h;
参考文献
Arai, Shigeru; Sudo, Yukinori; Nishida, Atsushi
Tetrahedron, 2005 , vol. 61, # 19 p. 4639 - 4642
反应条件
trifluoromethanesulfonic acid 2-pyridinyl ester; trifluoroacetic acid 5 h; Heating;
参考文献
Keumi, Takashi; Yoshimura, Kiichiro; Shimada, Masakazu; Kitajima, Hidehiko
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 455 - 460
反应条件
1: in tetrahydrofuran T=0°C; Green chemistry; 2: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione RefluxGreen chemistry;
参考文献
Sagara, Prateep Singh; Chebolu, Rajesh; Bahuguna, Ashish; Ravikumar
RSC Advances, 2014 , vol. 4, # 29 p. 15011 - 15013
反应条件
[2,2']bipyridinyl; sulfuric acid; water; palladium diacetate in 2-methyl-propan-1-ol T=100°C; 6 h; Inert atmosphere;
参考文献
Miao, Tao; Wang, Guan-Wu
Chemical Communications, 2011 , vol. 47, # 33 p. 9501 - 9503
反应条件
potassium phosphate; PdCl(NH2C6H4C6H4)(C6H4(CH3)4O3PC6H5); water in 2-methyl tetrahydrofuran T=60°C; 20 h; Inert atmosphere;
参考文献
Schmink, Jason R.; Krska, Shane W.
Journal of the American Chemical Society, 2011 , vol. 133, # 49 p. 19574 - 19577
反应条件
triethanolamine; palladium diacetate T=120°C; 0.166667 h; Inert atmosphereMicrowave irradiation;
参考文献
Silveira, Claudio C.; Larghi, Enrique L.; Mendes, Samuel R.; Bracca, Andrea B. J.; Rinaldi, Francieli; Kaufman, Teodoro S.
European Journal of Organic Chemistry, 2009 , # 27 p. 4637 - 4645
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium acetate; potassium carbonate; N-[2'-(dicyclohexylphosphino)-1,1'-biphenyl-2-yl]-N,N-dimethylamine in N,N-dimethyl acetamide T=110°C; 23 h; Inert atmosphere;
参考文献
Silveira, Claudio C.; Larghi, Enrique L.; Mendes, Samuel R.; Bracca, Andrea B. J.; Rinaldi, Francieli; Kaufman, Teodoro S.
European Journal of Organic Chemistry, 2009 , # 27 p. 4637 - 4645
反应条件
potassium fluoride; 18-crown-6 ether; 3-(2,4,6-trimethyl-phenyl)-5,6,7,8-tetrahydro-4H-cycloheptathiazol-3-ium perchlorate; potassium tert-butylate in tetrahydrofuran T=25°C; 6 h; Inert atmosphere;
参考文献
Biju, Akkattu T.; Glorius, Frank
Angewandte Chemie - International Edition, 2010 , vol. 49, # 50 p. 9761 - 9764
反应条件
aluminium trichloride
参考文献
Celgene Corporation
Patent: US5929117 A1, 1999 ;
