in hexane
byproducts: LiCl; all manipulations without O2 and moisture; Li compd. suspended in hexane, cooled to -78°C, Me3SnCl added by stirring, allowed to warm to room temp.; filtered, solvent removed in vac.;
参考文献
Wrackmeyer, Bernd; Pedall, Andreas; Weidinger, Juergen
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2001 , vol. 56, # 10 p. 1009 - 1014
1: phosphorus trichloride / diethyl ether / -5 °C
2: 100 percent / diethyl ether / 6 h / Ambient temperature
3: 36 percent / 150 - 180 °C / 0.02 Torr
View Scheme
参考文献
Markovskii, L.N.; Romanenko, V. D.; Klebanskii, E. O.; Povolotskii, M. I.; Chernega, A. N.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 8 p. 1721 - 1737,1524 - 1537