4-氟-N-[苄氧羰基]-DL-苯丙氨酸合成路线 （共 2 条）
反应条件
1: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride; 4-dimethylaminopyridine / CH2Cl2 2: HBr / acetic acid 3: Aspergillus oryzae protease; aq. NaOH / aq. phosphate buffer / 3.83 h / 30 °C / pH 7.0 View Scheme
参考文献
Miyazawa, Toshifumi; Imagawa, Kiwamu; Minowa, Hiroe; Miyamoto, Toyoko; Yamada, Takashi
Tetrahedron, 2005 , vol. 61, # 43 p. 10254 - 10261
反应条件
1: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride; 4-dimethylaminopyridine / CH2Cl2 2: 96 percent / HBr / acetic acid 3: Aspergillus oryzae protease; aq. NaOH / aq. phosphate buffer / 0.42 h / 30 °C / pH 7.0 View Scheme
参考文献
Miyazawa, Toshifumi; Imagawa, Kiwamu; Minowa, Hiroe; Miyamoto, Toyoko; Yamada, Takashi
Tetrahedron, 2005 , vol. 61, # 43 p. 10254 - 10261
